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ASTM-F1710:2008 Edition

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F1710-08 Standard Test Method for Trace Metallic Impurities in Electronic Grade Titanium by High Mass-Resolution Glow Discharge Mass Spectrometer

Published By Publication Date Number of Pages
ASTM 2008 6
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1.1 This test method covers the determination of concentrations of trace metallic impurities in high purity titanium.

1.2 This test method pertains to analysis by magnetic-sector glow discharge mass spectrometer (GDMS).

1.3 The titanium matrix must be 99.9 weight % (3 N -grade) pure, or purer, with respect to metallic impurities. There must be no major alloy constituent, for example, aluminum or iron, greater than 1000 weight ppm in concentration.

1.4 This test method does not include all the information needed to complete GDMS analyses. Sophisticated computer-controlled laboratory equipment skillfully used by an experienced operator is required to achieve the required sensitivity. This test method does cover the particular factors (for example, specimen preparation, setting of relative sensitivity factors, determination of sensitivity limits, etc.) known by the responsible technical committee to effect the reliability of high purity titanium analyses.

1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

PDF Catalog

PDF Pages PDF Title
1 Scope
Referenced Documents
Terminology
Summary of the Test Method
2 Significance and Use
Apparatus
Reagents and Materials
Preparation of Reference Standards and Test Specimens
3 Preparation of the GDMS Apparatus
Instrument Quality Control
TABLE 1
4 Standardization
Procedure
Detection Limit Determination
TABLE 2
5 GDMS Analysis for Thorium, Uranium, and Similar Elements
Report
FIG. 1
FIG. 2
6 Precision and Bias
Keywords
A1. MASS SPECTRUM INTERFERENCES FOR TITANIUM ANALYSIS BY GDMS
A1.1
ASTM-F1710
$40.63