{"id":338077,"date":"2024-10-19T23:38:59","date_gmt":"2024-10-19T23:38:59","guid":{"rendered":"https:\/\/pdfstandards.shop\/product\/uncategorized\/bs-en-12393-12013\/"},"modified":"2024-10-25T22:44:51","modified_gmt":"2024-10-25T22:44:51","slug":"bs-en-12393-12013","status":"publish","type":"product","link":"https:\/\/pdfstandards.shop\/product\/publishers\/bsi\/bs-en-12393-12013\/","title":{"rendered":"BS EN 12393-1:2013"},"content":{"rendered":"<p>This European Standard gives general considerations for the determination of pesticide residues in foods of plant origin.<\/p>\n<p>Each method specified in this European Standard is suitable for identifying and quantifying a definite range of those organohalogen, and\/or organophosphorus and\/or organonitrogen pesticides which occur as residues in foodstuffs of plant origin.<\/p>\n<p>This European Standard contains the following methods that have been subjected to interlaboratory studies and\/or are adopted throughout Europe:<\/p>\n<ul>\n<li>\n<p>method M: Extraction with acetone and liquid-liquid partition with dichloromethane\/light petroleum, if necessary clean-up on Florisil\u00ae <sup>1)<\/sup> [1], [2], [3];<\/p>\n<\/li>\n<li>\n<p>method N: Extraction with acetone, liquid-liquid partition with dichloromethane or cyclohexane\/ethyl acetate and clean-up with gel permeation and silica gel chromatography [4], [5];<\/p>\n<\/li>\n<li>\n<p>method P: Extraction with ethyl acetate and, if necessary, clean-up with gel permeation chromatography [6].<\/p>\n<\/li>\n<\/ul>\n<p>The applicability of the three methods M, N and P for residue analysis of organohalogen, organophosphorus and organonitrogen pesticides, respectively, is given for each method.<\/p>\n<h4>PDF Catalog<\/h4>\n<table border=\"1px\" class=\"des-table\">\n<tr>\n<th>PDF Pages<\/th>\n<th>PDF Title<\/th>\n<\/tr>\n<tr>\n<td><b>7<b><\/td>\n<td>1 Scope <br \/> 2 Normative references <br \/> 3 Principle <br \/> 3.1 General  <\/td>\n<\/tr>\n<tr>\n<td><b>8<b><\/td>\n<td>3.2 Extraction <br \/> 3.3 Clean-up <br \/> 3.4 Determination <br \/> 3.5 Confirmation <br \/> 3.6 Use of internal standards <br \/> 4 Reagents <br \/> 4.1 General  <\/td>\n<\/tr>\n<tr>\n<td><b>9<b><\/td>\n<td>4.2 Check for purity of reagents <br \/> 4.2.1 Solvents <br \/> 4.2.2 Water <br \/> 4.2.3 Inorganic salts <br \/> 4.2.4 Adsorbents <br \/> 4.2.5 Standard materials and solutions <br \/> 4.3 Safety aspects associated with reagents <br \/> 4.3.1 General  <\/td>\n<\/tr>\n<tr>\n<td><b>10<b><\/td>\n<td>4.3.2 Pesticides <br \/> 4.3.3 Hazardous reagents  <\/td>\n<\/tr>\n<tr>\n<td><b>11<b><\/td>\n<td>5 Apparatus <br \/> 5.1 Glassware: General  <\/td>\n<\/tr>\n<tr>\n<td><b>12<b><\/td>\n<td>5.2 Special glassware <br \/> 5.3 Auxiliary materials <br \/> 5.4 Solvent evaporators  <\/td>\n<\/tr>\n<tr>\n<td><b>13<b><\/td>\n<td>5.5 Homogenizers <br \/> 5.6 Centrifuges <br \/> 5.7 Gas chromatography <br \/> 5.8 Liquid chromatography <br \/> 6 Procedure <br \/> 6.1 General <br \/> 6.2 Small scale procedures  <\/td>\n<\/tr>\n<tr>\n<td><b>14<b><\/td>\n<td>6.3 Preparation and storage of the samples <br \/> 6.3.1 General <br \/> 6.3.2 Laboratory sample <br \/> 6.3.3 Partly-prepared test sample <br \/> 6.3.4 Test sample  <\/td>\n<\/tr>\n<tr>\n<td><b>15<b><\/td>\n<td>6.3.5 Test portion <br \/> 6.4 Extraction <br \/> 6.5 Clean-up <br \/> 7 Determination  <\/td>\n<\/tr>\n<tr>\n<td><b>16<b><\/td>\n<td>8 Confirmatory tests <br \/> 9 Evaluation of results <br \/> 9.1 Calculation  <\/td>\n<\/tr>\n<tr>\n<td><b>17<b><\/td>\n<td>9.2 Precision <br \/> 9.3 Practical limit of determination <br \/> 9.4 Expression of results <br \/> 10 Test report  <\/td>\n<\/tr>\n<tr>\n<td><b>18<b><\/td>\n<td>Annex A  (informative)  Purification of solvents and reagents  <\/td>\n<\/tr>\n<\/table>\n","protected":false},"excerpt":{"rendered":"<p><b>Foods of plant origin. Multiresidue methods for the determination of pesticide residues by GC or LC-MS\/MS &#8211; General considerations<\/b><\/p>\n<table class=\"shortdes-table\" style=\"width: 100%\" border=\"0\" cellspacing=\"0\" cellpadding=\"0\">\n<tbody>\n<tr>\n<td>Published By<\/td>\n<td>Publication Date<\/td>\n<td>Number of Pages<\/td>\n<\/tr>\n<tr>\n<td><a href=\"https:\/\/pdfstandards.shop\/product-category\/publishers\/bsi\/\"><b>BSI<\/b><\/a><\/td>\n<td>2013<\/td>\n<td>22<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n","protected":false},"featured_media":338083,"template":"","meta":{"rank_math_lock_modified_date":false,"ep_exclude_from_search":false},"product_cat":[2641],"product_tag":[],"class_list":{"0":"post-338077","1":"product","2":"type-product","3":"status-publish","4":"has-post-thumbnail","6":"product_cat-bsi","8":"first","9":"instock","10":"sold-individually","11":"shipping-taxable","12":"purchasable","13":"product-type-simple"},"_links":{"self":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product\/338077","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product"}],"about":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/types\/product"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media\/338083"}],"wp:attachment":[{"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/media?parent=338077"}],"wp:term":[{"taxonomy":"product_cat","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_cat?post=338077"},{"taxonomy":"product_tag","embeddable":true,"href":"https:\/\/pdfstandards.shop\/wp-json\/wp\/v2\/product_tag?post=338077"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}