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BS EN ISO 11357-1:2023

$167.15

Plastics. Differential scanning calorimetry (DSC) – General principles

Published By Publication Date Number of Pages
BSI 2023 44
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PDF Catalog

PDF Pages PDF Title
2 undefined
4 European foreword
Endorsement notice
7 Foreword
8 Introduction
9 1 Scope
2 Normative references
3 Terms and definitions
16 4 Basic principles
4.1 General
4.2 Heat-flux DSC
4.3 Power-compensation DSC
17 5 Apparatus and materials
18 6 Specimen
19 7 Test conditions and specimen conditioning
7.1 Test conditions
7.2 Conditioning of specimens
8 Calibration
8.1 General
20 8.2 Calibration materials
8.3 Temperature calibration
8.3.1 General
8.3.2 Procedure
21 8.3.3 Accuracy of calibration
8.4 Heat calibration
8.4.1 General
22 8.4.2 Procedure
8.4.3 Accuracy of calibration
8.5 Heat flow rate calibration
8.5.1 General
23 8.5.2 Procedure
25 9 Procedure
9.1 Setting up the apparatus
9.1.1 Switching on
9.1.2 Purge gas
9.1.3 Experimental conditions
9.1.4 Baseline determination
9.2 Loading the specimen into the crucible
9.2.1 General
9.2.2 Selection of crucibles
26 9.2.3 Weighing the specimen crucible
9.2.4 Loading the specimen
9.2.5 Determination of the mass of the specimen
9.3 Insertion of crucibles into the instrument
9.4 Performing measurements
9.4.1 General
9.4.2 Scanning mode
27 9.4.3 Isothermal mode
28 9.5 Post-run checks
9.5.1 Check for loss in mass
9.5.2 Inspection of specimens
9.5.3 Checking of crucibles and crucible holder
10 Test report
30 Annex A (normative) Extended, high-precision, temperature calibration[12]
32 Annex B (normative) Extended, high-precision, heat calibration
34 Annex C (informative) Recommended calibration materials
38 Annex D (informative) Interaction of calibration materials with different crucible materials
40 Annex E (informative) General recommendations
42 Bibliography
BS EN ISO 11357-1:2023
$167.15