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BS ISO 14411-2:2020

$142.49

Preparation of particulate reference materials – Polydisperse spherical particles

Published By Publication Date Number of Pages
BSI 2020 26
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This document describes the specifications for spherical polydisperse particulate reference materials with acceptable uncertainty in particle size distribution and describes protocols for their characterization. One potential use of these reference materials is the reliability test of the laser-diffraction instruments and other particle sizing methods.

This document expresses polydispersity and the related uncertainties in size. Small variations in size can imply large variations in cumulative distribution.

This document describes the requirements of particulate reference materials, which are intended to be used to test the reliability of various types of particle size measurement apparatus. The requirements for processing, homogeneity and stability assessment as well as for the preparation of certificates, which are not addressed in this document are described in ISO 17034.

PDF Catalog

PDF Pages PDF Title
2 undefined
6 Foreword
7 Introduction
9 1 Scope
2 Normative references
3 Terms, definitions and symbols
3.1 Terms and definitions
10 3.2 Symbols
11 4 Requirements for preparing polydisperse particles
4.1 General description of a project for the production of a reference material
12 4.2 Requirements on the general properties of the material for polydisperse particles
4.3 Size distribution for polydisperse particles
13 5 Characterization of polydisperse particles
5.1 Particle size distribution
5.2 Aspect ratio
5.3 Apparent particle density
5.4 Refractive index
6 Estimation of size measurement uncertainties
6.1 Uncertainty from sampling
6.1.1 Uncertainty of the average value N replicate measurement
14 6.1.2 Uncertainty of a single measurement
15 6.2 Other uncertainty factors
6.3 Expanded uncertainty of size distribution
16 Annex A (informative) Example calculation of the uncertainty estimation of particle size distribution determined by N replicate measurement
19 Annex B (informative) Example calculation of the uncertainty estimation of number-based particle size distribution determined by a single measurement
22 Annex C (informative) Example calculation of the uncertainty estimation for a volume-based cumulative size distribution transformed from the number-based size distribution having a log-normal size distribution
24 Bibliography
BS ISO 14411-2:2020
$142.49