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BSI PD IEC/TS 62607-4-1:2014

$102.76

Nanomanufacturing. Key control characteristics – Cathode nanomaterials for lithium ion batteries. Electrochemical characterisation, 2-electrode cell method

Published By Publication Date Number of Pages
BSI 2014 22
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This part of IEC 62607 provides a standardized method for the determination of electrochemical properties of lithium ion battery cathode nanomaterials to enable customers to:

  1. decide whether or not a cathode nanomaterial is usable, and

  2. select a cathode nanomaterial suitable for their application.

This technical specification includes:

  • definitions of terminology used in this document,

  • recommendations for sample preparation,

  • outlines of the experimental procedures used to measure cathode nanomaterial properties,

  • methods of interpretation of results and discussion of data analysis,

  • case studies and

  • references.

PDF Catalog

PDF Pages PDF Title
4 CONTENTS
5 FOREWORD
7 INTRODUCTION
8 1 Scope
2 Normative references
3 Terms, definitions, acronyms and abbreviations
3.1 Terms and definitions
9 3.2 Acronyms and abbreviations
4 Sample preparation methods
4.1 General
10 4.2 Reagents
4.2.1 Cathode foil
4.2.2 Anode
4.2.3 Solvents and separator
4.3 Pre-treatment of the cathode nanomaterial
11 4.4 Preparation of the screw cell
Tables
Table 1 – Spring force and pressure
12 4.5 Disassembly of the screw cell
5 Measurement of electrochemical properties
5.1 General
5.2 Open circuit voltage (OCV)
5.2.1 Demarcation of method
5.2.2 Experimental procedures and measurement conditions
5.3 Potentiostatic electrochemical impedance spectroscopy (EIS)
5.3.1 Demarcation of method
5.3.2 Experimental procedures and measurement conditions
5.4 Charge discharge experiment (constant current constant voltage, CCCV)
5.4.1 Demarcation of method
13 5.4.2 Experimental procedures and measurement conditions
6 Data analysis / Interpretation of results
6.1 Open circuit potential
6.2 Electrochemical impedance spectroscopy
6.3 Constant current constant voltage (CCCV) charging-discharging
14 Annex A (informative) Case study
A.1 Sample preparation
Figures
Figure A.1 – Components for the cell
16 Figure A.2 – Construction steps (a to g)
17 A.2 Results for a LCO electrode
Figure A.3 – Open circuit voltage/potential time graph
Figure A.4 – Electrochemical impedance graph
18 Figure A.5 – Constant current / constant voltage – Charge / Discharge
19 Figure A.6 – Capacity per cycle
BSI PD IEC/TS 62607-4-1:2014
$102.76